Fine chemical analysis

Author: Gao Kунюэ
Publisher:
Publish Date: 2002-08-01
Features: Introduction
The "Modern Analysis Test Technology Application Series" consists of four volumes, each introducing the current status and development trends of modern analysis test technologies in four fields: food testing, pharmaceutical analysis, environment, and fine chemical analysis. This book provides a comprehensive introduction to modern analysis test technologies commonly used in the fine chemical industry. In addition to general basic principles, it focuses on practical methods and actual applications of these technologies. It includes: ultraviolet spectroscopy, infrared spectroscopy, high-performance liquid chromatography, chromatography-mass spectrometry (LC-MS), and nuclear magnetic resonance (NMR) spectroscopy. It also provides a general introduction to powder diffraction. The content of this book incorporates the work experience and some achievements of the authors. It holds high reference value for scientific and technical personnel engaged in the analysis and research of fine chemical products, and can also be used as a reference for teachers and students in colleges and universities.
Table of Contents
Chapter 1 Introduction
Chapter 2 Ultraviolet-Visible Absorption Spectroscopy
Section 1 Principles and Applications of Ultraviolet-Visible Absorption Spectroscopy
Section 2 Ultraviolet-Visible Spectrophotometer
Section 3 Experimental Techniques
Section 4 Factors Affecting Ultraviolet-Visible Absorption Spectra
Section 5 Application of Ultraviolet-Visible Absorption Spectra in Qualitative Identification of Compounds
Section 6 Application of Ultraviolet-Visible Absorption Spectra in Quantitative Analysis
Chapter 3 Infrared Spectroscopy
Section 1 Overview
Section 2 Infrared Spectrophotometer
Section 3 Characteristic Frequencies of Functional Groups in Organic Molecules
Section 4 Experimental Techniques
Section 5 Applications of Infrared Spectroscopy
Section 6 Case Studies
Chapter 4 High-Performance Liquid Chromatography
Section 1 Overview
Section 2 High-Performance Liquid Chromatograph
Section 3 Role of Mobile and Stationary Phases
Section 4 Method Development
Section 5 Case Studies
Chapter 5 Gas Chromatography-Mass Spectrometry (GC-MS)
Section 1 Overview
Section 2 GC-MS Instrument
Section 3 Chromatography Columns
Section 4 Mass Spectrum and Interpretation
Section 5 Method Development
Section 6 Routine Maintenance
Section 7 Case Studies
Chapter 6 Liquid Chromatography-Mass Spectrometry (LC-MS)
Section 1 Overview
Section 2 Atmospheric Pressure Ionization Techniques
Section 3 Method Optimization
Section 4 Spectrum Interpretation
Section 5 Applications of LC-MS
Chapter 7 Nuclear Magnetic Resonance (NMR) Spectroscopy
Section 1 Basic Principles
Section 2 Proton NMR and Spectrum Interpretation
Section 3 Carbon NMR
Section 4 Two-Dimensional NMR
Section 5 NMR Instruments and Experimental Methods
Section 6 Applications of NMR
Chapter 8 Powder Diffraction
Section 1 Overview and Basic Knowledge
Section 2 Powder Diffraction Instrument
Section 3 Sample Preparation Techniques
Section 4 Establishment of General Phase Analysis Experimental Methods
Section 5 Principles and Methods of Qualitative Phase Analysis
Section 6 Case Studies
Chapter 9 Comprehensive Application Examples
Section 1 Selection of Different Analysis and Test Methods Based on the Structural Characteristics of Compounds
Section 2 Comparison of Different Analysis and Test Methods
Section 3 Identification of Complex Mixtures