Instrumental analysis techniques

Author: Wang Xiuping
Publisher:
Publish Date: 2003-01-01
Features: This book is one of the "Practical Technology Readers for Worker Training." It is divided into 20 chapters, covering topics such as gas chromatography, high-performance liquid chromatography, ion chromatography, gel permeation chromatography, supercritical fluid chromatography, capillary electrophoresis, atomic absorption spectroscopy, atomic emission spectroscopic analysis, X-ray diffraction analysis, X-ray fluorescence spectroscopy, an introduction to X-ray photoelectron spectroscopy, electron microscopy, ultraviolet and visible spectrophotometry, electrochemical analysis, thermal analysis, flow injection analysis, nuclear magnetic resonance, organic mass spectrometry, infrared spectroscopy, and Raman spectroscopy, as well as on-line analysis methods. The book provides detailed explanations of common analytical methods and instruments while also including numerous practical examples. It is rich in content and highly practical. This book can serve as a training textbook for technical workers or self-study materials, and is also suitable for engineers, technicians, and management personnel.
Table of Contents
Chapter 1 Introduction
1. Overview
2. Classification of Instrumental Analysis Methods
3. Characteristics of Instrumental Analysis
Chapter 2 Gas Chromatography
1. Overview
2. Basic Terminology
3. Basic Instrument Structure
4. Selection of Chromatographic Conditions
5. Operation Precautions for Gas Chromatographs
6. Qualitative and Quantitative Analysis by Gas Chromatography
7. Sample Introduction Methods
8. Sample Pretreatment
9. Preparation of Packing Columns
10. Applications
Chapter 3 High-Performance Liquid Chromatography
1. Overview
2. Classification and Selection of Liquid Chromatography
3. Instrumentation
4. Mobile Phase for Liquid Chromatography
5. Adsorption Chromatography
6. Partition Chromatography
7. Establishment of Liquid Chromatography Methods
8. Precautions in Liquid Chromatography Operation
9. Daily Maintenance of HPLC
10. Applications
Chapter 4 Ion Chromatography
1. Overview
2. Ion Exchange Chromatography
3. Ion Exclusion Chromatography
4. Ion Pair Chromatography
5. Interferences in Ion Chromatography
6. Issues to Note in Ion Chromatography Analysis
7. Applications
Chapter 5 Gel Permeation Chromatography
1. Overview
2. Separation Principles and Characteristics
3. Average Relative Molecular Weight and Molecular Weight Distribution
4. Instrumentation
5. Stationary and Mobile Phases
6. Data Processing for Gel Permeation Chromatography
7. Factors Affecting Gel Permeation Chromatography Results
8. Maintenance of Chromatography Columns
9. Applications
Chapter 6 Supercritical Fluid Chromatography
1. Overview
2. Principles of Supercritical Fluid Chromatography
3. Instrumentation
4. Applications of SFC
5. Supercritical Fluid Extraction
Chapter 7 Capillary Electrophoresis
1. Overview
2. Basic Principles of Electrophoresis
3. Capillary Electrophoresis Systems
4. Basic Operations and Selection of Separation Conditions
5. Applications
Chapter 8 Atomic Absorption Spectroscopy
1. Overview
2. Relationship Between Atomic Absorption and Atomic Concentration
3. Composition of Atomic Absorption Spectrometers
4. Selection of Measurement Conditions
5. Quantitative Methods for Atomic Absorption Spectroscopy
6. Interferences and Their Elimination
7. Sample Handling
8. Applications
Chapter 9 Atomic Emission Spectroscopic Analysis
1. Overview
2. Principles
3. Instrumentation
4. Qualitative Analysis
5. Quantitative Analysis
6. Methods of Sample Introduction and Excitation by Light Sources
7. Inductively Coupled Plasma Emission Spectroscopy
Chapter 10 X-Ray Diffraction Analysis and X-Ray Fluorescence Spectroscopy
1. Overview
2. X-Ray Diffraction Analysis
3. X-Ray Fluorescence Spectroscopy
4. Comparison Between X-Ray Diffraction and X-Ray Fluorescence Analysis
Chapter 11 Introduction to X-Ray Photoelectron Spectroscopy
1. Overview
2. Principles of X-Ray Photoelectron Spectroscopy
3. Chemical Shifts in X-Ray Photoelectron Spectroscopy
4. Experimental Methods for X-Ray Photoelectron Spectroscopy
5. Work Content of X-Ray Photoelectron Spectroscopy
6. Examples of Applications of X-Ray Photoelectron Spectroscopy
Chapter 12 Electron Microscopic Analysis
1. Overview
2. Transmission Electron Microscopy
3. Scanning Electron Microscopy
4. Scanning Tunneling and Atomic Force Electron Microscopy
Chapter 13 Ultraviolet and Visible Spectrophotometry
1. Overview
2. Visible Spectrophotometry
3. Ultraviolet Spectrophotometry
Chapter 14 Electrochemical Analysis
1. Overview
2. Classification of Electrochemical Analysis Methods
3. Potentiometric Analysis
4. Coulometric Analysis
5. Conductometric Analysis
Chapter 15 Thermal Analysis
1. Overview
2. Composition of Thermal Analyzers
3. Thermogravimetric Analysis
4. Differential Thermal Analysis
5. Differential Scanning Calorimetry
6. Precautions for Determinations
Chapter 16 Flow Injection Analysis
1. Overview
2. Principles of Flow Injection Analysis
3. Instrumentation
4. Applications
Chapter 17 Nuclear Magnetic Resonance Spectroscopy
1. Basic Principles of Nuclear Magnetic Resonance
2. Nuclear Magnetic Resonance Instruments
3. Chemical Shifts
4. Nuclear Magnetic Resonance Hydrogen Spectrum
5. Spin Coupling and Splitting
6. Common Spin Systems
7. Simplified Experimental Methods for Nuclear Magnetic Hydrogen Spectrum
8. Interpretation of Nuclear Magnetic Hydrogen Spectrum
9. Nuclear Magnetic Carbon Spectrum
Chapter 18 Organic Mass Spectrometry
1. Basic Knowledge of Organic Mass Spectrometry
2. Main Types of Molecular Ions in Organic Mass Spectrometry
3. Mass Spectra of Common Organic Compounds
4. Identification and Application of Isotope Peaks
5. Determination of Element Composition in Molecules from Low-Resolution Mass Spectra
6. Calculation and Application of Molecular Formula Unsaturation
7. Interpretation of Mass Spectra and Structure Prediction
8. Examples of Mass Spectral Interpretation
Chapter 19 Infrared Spectroscopy and Raman Spectroscopy
1. Basic Principles of Infrared Spectroscopy
2. Vibrations and Vibrational Spectra
3. Molecular Vibrational Modes in Infrared Spectroscopy
4. Characteristic Frequencies of Various Functional Groups
5. Factors Affecting the Absorption Frequencies of Functional Groups
6. Interpretation of Infrared Spectra
7. Quantitative Analysis by Infrared Spectroscopy
8. Infrared Spectrometers and Sample Preparation Methods
9. Infrared Photoacoustic Spectroscopy
10. Raman Spectroscopy
Chapter 20 On-Line Analysis Methods
1. Gas Chromatography-Mass Spectrometry (GC-MS)
2. Liquid Chromatography-Mass Spectrometry (LC-MS)
3. Chromatography-Fourier Transform Infrared Spectroscopy (FTIR)
4. GC/MS/FTIR